diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

Base Information

Chemical Name:diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate
CAS No.:1202246-58-9
Molecular Formula:C₂₉H₃₀NO₅PS
Molecular Weight:535.601
Hs Code.:

Synonyms:diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

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Chemical Property of diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

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Technology Process of diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

There total 2 articles about diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 327175-79-1
N-(1-phenylethylidene)-2,4,6-trimethylphenylsulfonamide

: 4712-55-4
diphenyl hydrogen phosphite

: 1202246-58-9
diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

Guidance literature:: With sodium carbonate; dihydroquinine; In toluene; at -20 ℃; for 60h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja908940e

Reference yield:

: 327175-79-1
N-(1-phenylethylidene)-2,4,6-trimethylphenylsulfonamide

: 4712-55-4
diphenyl hydrogen phosphite

: 1202246-63-6
diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

: 1202246-58-9
diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

Guidance literature:: With sodium carbonate; quinine; In toluene; at 20 ℃; for 27h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja908940e

Reference yield: 96.0%

: 1202246-58-9
diphenyl 1-(2,4,6-trimethylphenylsulfonylamino)-1-phenylethylphosphonate

: 1202247-05-9
diphenyl (S)-1-amino-1-phenylethylphosphonate

Guidance literature:: With methanesulfonic acid; methyl-phenyl-thioether; trifluoroacetic acid; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja908940e