C₁₅H₁₂FNO

Base Information

Chemical Name:C₁₅H₁₂FNO
CAS No.:1350705-00-8
Molecular Formula:C₁₅H₁₂FNO
Molecular Weight:241.265
Hs Code.:

Synonyms:C₁₅H₁₂FNO

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Chemical Property of C₁₅H₁₂FNO

Chemical Property:

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Technology Process of C₁₅H₁₂FNO

There total 3 articles about C₁₅H₁₂FNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 352-34-1
4-fluoro-1-iodobenzene

: 52536-39-7
2-(prop-2-ynyloxy)benzenediazonium tetrafluoroborate

: 1350705-00-8
C₁₅H₁₂FNO

Guidance literature:: 4-fluoro-1-iodobenzene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; for 0.333333h; Inert atmosphere;

2-(prop-2-ynyloxy)benzenediazonium tetrafluoroborate; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1ob06353g

Reference yield:

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 1350705-00-8
C₁₅H₁₂FNO

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 3 h / 20 °C

1.2: 9 h / Reflux

2.1: iron; acetic acid / 8 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.33 h / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iron; potassium carbonate; acetic acid; triethylamine; In acetone; 3.1: Sonogashira coupling / 3.2: Sonogashira coupling;
DOI:10.1039/c1ob06353g

Reference yield:

: 13350-09-9
1-nitro-2-(prop-2-yn-1-yloxy)benzene

: 1350705-00-8
C₁₅H₁₂FNO

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron; acetic acid / 8 h / 20 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.33 h / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iron; acetic acid; triethylamine; 2.1: Sonogashira coupling / 2.2: Sonogashira coupling;
DOI:10.1039/c1ob06353g