2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

Base Information

Chemical Name:2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol
CAS No.:222723-43-5
Molecular Formula:C₃₃H₄₂O₆Si
Molecular Weight:562.778
Hs Code.:

Synonyms:2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

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Technology Process of 2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

There total 3 articles about 2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 222408-63-1
3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

: 222723-43-5
2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

Guidance literature:: With dmap; In pyridine; for 3h;
DOI:10.1080/07328309908543990

Reference yield:

: 106929-09-3
(2S,3R,4R)-2,3-dibenzyloxy-4,5-isopropylidenedioxypentanal

: 222723-43-5
2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0 °C

2: 100 percent / DMAP / pyridine / 3 h

With dmap; In pyridine; diethyl ether;
DOI:10.1080/07328309908543990

Reference yield:

: 175606-34-5
2,3-di-O-benzyl-4,5-O-isopropylidene-D-arabinose diethyl dithioacetal

: 222723-43-5
2-O-acetyl-3,4-di-O-benzyl-5,6-O-isopropylidene-1-deoxy-1-dimethylphenylsilyl-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: HgO, BF₃*Et₂O / tetrahydrofuran; H₂O

2: diethyl ether / 0 °C

3: 100 percent / DMAP / pyridine / 3 h

With dmap; boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; pyridine; diethyl ether; water;
DOI:10.1080/07328309908543990