3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

Base Information

Chemical Name:3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol
CAS No.:222408-63-1
Molecular Formula:C₃₁H₄₀O₅Si
Molecular Weight:520.741
Hs Code.:

Synonyms:3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

Chemical Property:

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Technology Process of 3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

There total 4 articles about 3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107735-20-6
[(dimethylphenylsilyl)methyl]magnesium chloride

: 106929-09-3
(2S,3R,4R)-2,3-dibenzyloxy-4,5-isopropylidenedioxypentanal

: 222408-63-1
3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

Guidance literature:: In diethyl ether; at 0 ℃; for 2h;
DOI:10.1080/07328309908543989

Reference yield:

: 1941-50-0
D-arabinose diethyl dithioacetal

: 222408-63-1
3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium p-toluenesylfonate / acetone

2: NaH / tetrahydrofuran / 0 °C

3: HgO, BF₃*Et₂O / tetrahydrofuran; H₂O / 0.5 h

4: 7.0 g / diethyl ether / 2 h / 0 °C

With boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; sodium hydride; mercury(II) oxide; In tetrahydrofuran; diethyl ether; water; acetone;
DOI:10.1080/07328309908543989

Reference yield:

: 100-39-0
benzyl bromide

: 222408-63-1
3,4-di-O-benzyl-1-deoxy-1-dimethylphenylsilyl-5,6-O-isopropylidene-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran / 0 °C

2: HgO, BF₃*Et₂O / tetrahydrofuran; H₂O / 0.5 h

3: 7.0 g / diethyl ether / 2 h / 0 °C

With boron trifluoride diethyl etherate; sodium hydride; mercury(II) oxide; In tetrahydrofuran; diethyl ether; water;
DOI:10.1080/07328309908543989