C₃₉H₇₆O₅Si₃

Base Information

• Chemical Name: C₃₉H₇₆O₅Si₃
• CAS No.: 1266621-74-2
• Molecular Formula: C₃₉H₇₆O₅Si₃
• Molecular Weight: 709.286
• Mol file: 1266621-74-2.mol

Synonyms:C₃₉H₇₆O₅Si₃

Chemical Property of C₃₉H₇₆O₅Si₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₃₉H₇₆O₅Si₃

There total 6 articles about C₃₉H₇₆O₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C39H74O5Si3 → C39H76O5Si3 (1266621-74-2)

Guidance literature:

With hydrogen; In ethyl acetate; for 18h; under 760.051 Torr;

DOI:10.1002/chem.201002501

Reference yield:

triethylsilyl chloride (994-30-9) → C39H76O5Si3 (1266621-74-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 0 °C

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / Inert atmosphere; Reflux

3: hydrogen / ethyl acetate / 18 h / 760.05 Torr

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogen; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1002/chem.201002501

Reference yield:

C19H32O2Si (1266621-77-5) → C39H76O5Si3 (1266621-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / Inert atmosphere; Reflux

2: hydrogen / ethyl acetate / 18 h / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogen; In dichloromethane; ethyl acetate;

DOI:10.1002/chem.201002501

upstream raw materials:

C₁₉H₃₂O₂Si

C₂₂H₄₆O₃Si₂

triethylsilyl chloride

(2R,3S)-1-Benzyloxy-3-methyl-pent-4-en-2-ol

Downstream raw materials:

C₂₇H₄₆O₄Si

C₂₇H₄₆O₄Si

C₂₁H₃₂O₄

C₂₁H₃₂O₄