[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

Base Information

Chemical Name:[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid
CAS No.:101575-64-8
Molecular Formula:C₁₇H₁₈N₂O₇
Molecular Weight:362.339
Hs Code.:

[(3<i>S</i>)-2<i>t</i>-carboxy-4<i>c</i>-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3<i>r</i>-yl]-acetic acid

Synonyms:[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

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Chemical Property of [(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

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Technology Process of [(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

There total 3 articles about [(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 487-79-6
(-)-kainic acid

: 122-04-3
4-nitro-benzoyl chloride

: 101575-64-8
[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

Guidance literature:: With sodium hydroxide; In water; at 0 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/chem.201406557

Reference yield:

: C₂₃H₃₃NO₆

: 101575-64-8
[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid; triethylsilane / 13 h / Inert atmosphere; Reflux

2: sodium hydroxide / water / 20 h / 0 - 20 °C / Inert atmosphere

With triethylsilane; trifluoroacetic acid; sodium hydroxide; In water;
DOI:10.1002/chem.201406557

Reference yield:

: C₂₃H₃₅NO₅

: 101575-64-8
[(3S)-2t-carboxy-4c-isopropenyl-1-(4-nitro-benzoyl)-pyrrolidin-3r-yl]-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: chromium(VI) oxide; periodic acid / water; acetonitrile / 8.5 h / 0 °C / Inert atmosphere

2: trifluoroacetic acid; triethylsilane / 13 h / Inert atmosphere; Reflux

3: sodium hydroxide / water / 20 h / 0 - 20 °C / Inert atmosphere

With chromium(VI) oxide; triethylsilane; periodic acid; trifluoroacetic acid; sodium hydroxide; In water; acetonitrile; 1: |Jones Oxidation;
DOI:10.1002/chem.201406557