Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

Base Information

Chemical Name:Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate
CAS No.:198631-35-5
Molecular Formula:C₁₉H₂₅BrO₃
Molecular Weight:381.31
Hs Code.:

Synonyms:Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

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Technology Process of Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

There total 3 articles about Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 917-54-4
methyllithium

: 150270-93-2
Ethyl 3-<2-(2-bromophenyl)ethyl>-2-methyl-4-oxocyclohex-2-enecarboxylate

: 198631-35-5
Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

Guidance literature:: With copper(l) iodide; boron trifluoride diethyl etherate; In diethyl ether; 1.) -50 deg C, 5 min, 2.) -30 deg C, 75 min;

Reference yield:

: 487-51-4
4-carbethoxy-3-methyl-2-cyclohexen-1-one

: 198631-35-5
Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / t-BuOK / 2-methyl-propan-2-ol

2: 88 percent / CuI, BF₃*Et₂O / diethyl ether / 1.) -50 deg C, 5 min, 2.) -30 deg C, 75 min

With copper(l) iodide; boron trifluoride diethyl etherate; potassium tert-butylate; In diethyl ether; tert-butyl alcohol;

Reference yield:

: 1074-15-3
1-bromo-2-(2-bromoethyl)benzene

: 198631-35-5
Ethyl 3-[2-(2-bromophenyl)ethyl]-2,2-dimethyl-4-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / t-BuOK / 2-methyl-propan-2-ol

2: 88 percent / CuI, BF₃*Et₂O / diethyl ether / 1.) -50 deg C, 5 min, 2.) -30 deg C, 75 min

With copper(l) iodide; boron trifluoride diethyl etherate; potassium tert-butylate; In diethyl ether; tert-butyl alcohol;