methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

Base Information

Chemical Name:methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate
CAS No.:886042-59-7
Molecular Formula:C₂₅H₂₈N₂O₂
Molecular Weight:388.51
Hs Code.:

Synonyms:methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

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Chemical Property of methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

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Technology Process of methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

There total 2 articles about methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 886042-58-6
methyl2-[2-(aminomethyl)phenyl]-3-cyclohexyl-1-(1,3-dioxolan-2-ylmethyl)-1H-indole-6-carboxylate

: 886042-59-7
methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

Guidance literature:: methyl2-[2-(aminomethyl)phenyl]-3-cyclohexyl-1-(1,3-dioxolan-2-ylmethyl)-1H-indole-6-carboxylate; With hydrogenchloride; water; In tetrahydrofuran; for 24h; Heating / reflux;

With acetic acid; In methanol; for 0.333333h; pH=4;

With water; sodium cyanoborohydride; sodium hydrogencarbonate; more than 3 stages;

Reference yield:

: 1132679-52-7
C₂₅H₂₆N₂O₃

: 886042-59-7
methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2008.12.068

Reference yield: 100.0%

: 25016-11-9
1-methylpyrazole-4-carbaldehyde

: 886042-59-7
methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

: 886043-72-7
methyl 14-cyclohexyl-6-[(1-methyl-1H-pyrazol-4-yl)methyl]-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate

Guidance literature:: 1-methylpyrazole-4-carbaldehyde; methyl 14-cyclohexyl-5,6,7,8-tetrahydroindolo[2,1-a][2,5]benzodiazocine-11-carboxylate; With acetic acid; In methanol; at 20 ℃; for 0.5h; pH=4;

With sodium cyanoborohydride; In methanol; at 20 ℃; for 16h;

With water; sodium hydrogencarbonate; In methanol;