1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane
CAS No.:1621595-72-9
Molecular Formula:C₂₂H₂₄B₁₀N₂O
Molecular Weight:440.555
Hs Code.:

Synonyms:1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Suppliers and Price of 1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

There total 3 articles about 1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1621595-64-9
1-(4-aminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

: 98-88-4
benzoyl chloride

: 1621595-72-9
1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1621595-72-9
1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; tetrahydrofuran / 3 h / 20 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With 10 wt% Pd(OH)2 on carbon; hydrogen; sodium hydride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield:

: 1621595-62-7
1-(4-cyanophenyl)-2-(4-nitrophenyl)-1,2-dicarba-closo-dodecaborane

: 1621595-72-9
1-(4-benzoylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: Multi-step reaction with 2 steps

1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; tetrahydrofuran / 3 h / 20 °C

2: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With 10 wt% Pd(OH)2 on carbon; hydrogen; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.07.034