2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

Base Information

Chemical Name:2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile
CAS No.:882696-38-0
Molecular Formula:C₂₆H₃₈BrNOS
Molecular Weight:492.564
Hs Code.:

Synonyms:2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

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Chemical Property of 2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

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Technology Process of 2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

There total 4 articles about 2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 882696-24-4
1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

: 882696-38-0
2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

Guidance literature:: With carbon tetrabromide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2006.01.161

Reference yield:

: 882696-23-3
2-{1-[chloro-(toluene-4-sulfinyl)-methyl]-cyclopentadecyl}-propionitrile

: 882696-38-0
2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tBuOK / tetrahydrofuran; 2-methyl-propan-2-ol / -78 - 20 °C

2: 85 percent / LDA; CBr₄ / tetrahydrofuran

With carbon tetrabromide; potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2006.01.161

Reference yield:

: 172467-97-9
[chloro-(p-tolylsulfinyl)methylidene]cyclopentadecane

: 882696-38-0
2-bromo-1-methyl-2-(toluene-4-sulfinyl)-spiro[2.14]heptadecane-1-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / tetrahydrofuran / 0.17 h / -78 °C

2: 90 percent / tBuOK / tetrahydrofuran; 2-methyl-propan-2-ol / -78 - 20 °C

3: 85 percent / LDA; CBr₄ / tetrahydrofuran

With carbon tetrabromide; potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2006.01.161