copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

Base Information

Chemical Name:copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole
CAS No.:444987-88-6
Molecular Formula:C₄₀H₁₂Br₈CuF₉N₄
Molecular Weight:1422.33
Hs Code.:

copper β-octabromo-meso-tris(p-CF<sub>3</sub>-phenyl)corrole

Synonyms:copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

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Chemical Property of copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

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Technology Process of copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

There total 3 articles about copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 444987-84-2
Cu(C₁₉H₈N₄(C₆H₄CF₃)3)

: 444987-88-6
copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

Guidance literature:: Cu(C₁₉H₈N₄(C₆H₄CF₃)3); With bromine; In chloroform; at 20 ℃; for 1h;

With pyridine; In chloroform; for 1h;
DOI:10.1016/j.jinorgbio.2015.07.017

Reference yield:

: 5,10,15-tris(p-trifluoromethylphenyl)corrole

: 444987-88-6
copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: sodium metabisulfite / water; chloroform; pyridine

With sodium metabisulfite; In pyridine; chloroform; water;
DOI:10.1021/ja0113697

Reference yield:

: 444987-84-2
Cu(C₁₉H₈N₄(C₆H₄CF₃)3)

: 7726-95-6
bromine

: 444987-88-6
copper β-octabromo-meso-tris(p-CF₃-phenyl)corrole

Guidance literature:: With sodium metabisulfite; In pyridine; chloroform; water; to stirred soln. of Cu(III)-complex in CHCl3 added Br2 dissolved in CHCl3 over 15 min at room temp.; mixt. stirred for 1 h; pyridine dissolved in CHCl3 added dropwise over 15 min; soln. stirred for 1 h; aq. soln. of sodium metabisulfite added; org. layer sepd.; dried (anhyd. Na2SO4); solvent evapd.; purified by chromy. on silica gel (hexane/CH2Cl2 as eluent);
DOI:10.1021/ja0113697