3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

Base Information

Chemical Name:3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine
CAS No.:1174063-88-7
Molecular Formula:C₃₇H₃₅N₃O₈
Molecular Weight:649.7
Hs Code.:

Synonyms:3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

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Chemical Property of 3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

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Technology Process of 3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

There total 7 articles about 3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1174063-91-2
3-(2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1174063-88-7
3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

Guidance literature:: With pyridine; at 20 ℃; for 3.5h;

Reference yield:

: 1393486-74-2
C₁₄H₁₆BrClN₂O₇

: 1174063-88-7
3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

2: cesium fluoride / ethanol / 24 h / Heating; Reflux

3: pyridine / 3.5 h / 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; cesium fluoride; In pyridine; ethanol; dichloromethane;

Reference yield:

: 1188522-81-7
3',5'-diacetyl-5-bromo-2'-O-methyluridine

: 1174063-88-7
3-(5'-O-dimethoxytrityl-2'-O-methyl-β-D-ribofuranosyl)-1,3-diaza-2-oxophenoxazine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrachloromethane; triphenylphosphine / dichloromethane / Heating; Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C

3: cesium fluoride / ethanol / 24 h / Heating; Reflux

4: pyridine / 3.5 h / 20 °C

With tetrachloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; cesium fluoride; In pyridine; ethanol; dichloromethane;