4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

Base Information

Chemical Name:4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride
CAS No.:1308254-67-2
Molecular Formula:C₁₄H₁₅BN₂O₅S*ClH
Molecular Weight:370.621
Hs Code.:

Synonyms:4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

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Chemical Property of 4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

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Technology Process of 4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

There total 3 articles about 4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1308255-81-3
N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

: 1308254-67-2
4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

Guidance literature:: N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide; With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 2h; under 2585.81 Torr;

With hydrogenchloride; In water;

Reference yield:

: 21320-91-2
2-methoxy-4-nitrobenzene-1-sulfonyl chloride

: 1308254-67-2
4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / acetonitrile / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 2 h / 20 °C / 2585.81 Torr

With pyridine; hydrogen; palladium 10% on activated carbon; In ethanol; acetonitrile;

Reference yield:

: 117098-94-9
(5-amino-2-hydroxymethylphenyl)boronic acid

: 1308254-67-2
4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / acetonitrile / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 2 h / 20 °C / 2585.81 Torr

With pyridine; hydrogen; palladium 10% on activated carbon; In ethanol; acetonitrile;