N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide
CAS No.:1308255-81-3
Molecular Formula:C₁₄H₁₃BN₂O₇S
Molecular Weight:364.143
Hs Code.:

Synonyms:N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

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Technology Process of N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

There total 1 articles about N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 21320-91-2
2-methoxy-4-nitrobenzene-1-sulfonyl chloride

: 117098-94-9
(5-amino-2-hydroxymethylphenyl)boronic acid

: 1308255-81-3
N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

Guidance literature:: With pyridine; In acetonitrile; at 20 ℃;

Reference yield: 83.0%

: 1308255-81-3
N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

: 1308255-82-4
2-hydroxy-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

Guidance literature:: With boron tribromide; In dichloromethane; at 20 ℃;

Reference yield: 13.0%

: 1308255-81-3
N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide

: 1308254-67-2
4-amino-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxybenzenesulfonamide hydrochloride

Guidance literature:: N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-2-methoxy-4-nitrobenzenesulfonamide; With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 2h; under 2585.81 Torr;

With hydrogenchloride; In water;