2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

Base Information

Chemical Name:2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide
CAS No.:848489-99-6
Molecular Formula:C₅₆H₅₆N₆O₁₀
Molecular Weight:973.095
Hs Code.:

2,3-bis-benzyloxy-<i>N</i>,<i>N</i>'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

Synonyms:2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

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Chemical Property of 2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

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Technology Process of 2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

There total 2 articles about 2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.2%

: 848490-02-8
3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carboxylic acid (3-amino-propyl)-amide

: 492454-84-9
(2,3-bis(benzyloxy)-1,4-phenylene)bis((2-thioxothiazolidin-3-yl)methanone)

: 848489-99-6
2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/ja061323j

Reference yield:

: 169237-39-2
3-(benzyloxy)-1-methyl-4-<(2-thioxothiazoldin-1-yl)carbonyl>-2(1H)-pyridinone

: 848489-99-6
2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 83.2 percent / CH₂Cl₂ / 5 h / 20 °C

2: 94.2 percent / triethylamine / CH₂Cl₂ / 48 h / 20 °C

With triethylamine; In dichloromethane;
DOI:10.1021/ja061323j

Reference yield: 98.6%

: 848489-99-6
2,3-bis-benzyloxy-N,N'-bis-{3-[(3-benzyloxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

: 2,3-dihydroxy-N,N'-bis-{3-[(3-hydroxy-1-methyl-2-oxo-1,2-dihydro-pyridine-4-carbonyl)-amino]-propyl}-terephthalamide

Guidance literature:: With hydrogenchloride; water; hydrogen; palladium on activated charcoal; In acetic acid; at 20 ℃; for 72h;
DOI:10.1021/ja061323j