amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride

Base Information

• Chemical Name: amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride
• CAS No.: 1542782-36-4
• Molecular Formula: C₁₉H₃₂N₅O₂P*ClH
• Molecular Weight: 429.93

Synonyms:amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride

Chemical Property of amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride

Chemical Property:

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Technology Process of amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride

There total 1 articles about amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(benzyloxycarbonylamino)(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride (1542782-32-0) → amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride (1542782-36-4)

Guidance literature:

With triethylsilane; triethylamine; palladium dichloride; In dichloromethane; Inert atmosphere; Reflux;

DOI:10.1055/s-0033-1340058

Reference yield: 90.0%

amino(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride (1542782-36-4) → 2-(aminodi(pyrrolidin-1-yl)phosphonio)-2-phenylhydrazin-1-ium dibromide

Guidance literature:

With hydrogen bromide; In methanol; water; at 50 ℃; Inert atmosphere;

DOI:10.1055/s-0033-1340058

upstream raw materials:

(benzyloxycarbonylamino)(2-(tert-butoxycarbonyl)-1-phenylhydrazinyl)di(pyrrolidin-1-yl)phosphonium chloride

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