1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

Base Information

Chemical Name:1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol
CAS No.:81712-99-4
Molecular Formula:C₄₂H₄₄O₁₁S₂
Molecular Weight:788.937
Hs Code.:

Synonyms:1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

Chemical Property:

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Technology Process of 1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

There total 1 articles about 1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75348-12-8
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-chiro-inositol

: 98-59-9
p-toluenesulfonyl chloride

: 81712-99-4
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: With pyridine; at 60 ℃; for 12h;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield: 96.0%

: 81712-99-4
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

: 81713-01-1
1L-1,7-Anhydro-2,3,4-tri-O-benzyl-1-C-hydroxymethyl-5-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: With sodium methylate; In methanol; for 0.75h; Ambient temperature;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-99-4
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

: 1D-(1N,2,4/3)-1-Azido-5-C-azidomethyl-2,3,4-tri-O-benzyl-2,3,4-trihydroxycyclohex-5-en

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / sodium methoxide / methanol / 0.75 h / Ambient temperature

2: 79 percent / 3-methyl-2-selenoxobenzothiazole, trifluoroacetic acid / CH₂Cl₂ / 20 h / Ambient temperature

3: 91 percent / pyridine / 2 h / 20 °C

4: 81 percent / sodium azide / dimethylformamide / 1 h / 80 °C

With pyridine; sodium azide; N-methyl-1,3-benzothiazole-2(3H)-selone; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)88052-0