2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

Base Information

Chemical Name:2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol
CAS No.:81713-03-3
Molecular Formula:C₃₅H₃₆O₇S
Molecular Weight:600.733
Hs Code.:

Synonyms:2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

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Chemical Property of 2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

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Technology Process of 2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

There total 4 articles about 2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 81713-01-1
1L-1,7-Anhydro-2,3,4-tri-O-benzyl-1-C-hydroxymethyl-5-O-p-tolylsulfonyl-chiro-inositol

: 81713-03-3
2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: With N-methyl-1,3-benzothiazole-2(3H)-selone; trifluoroacetic acid; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 81712-99-4
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-5,7-di-O-p-tolylsulfonyl-chiro-inositol

: 81713-03-3
2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / sodium methoxide / methanol / 0.75 h / Ambient temperature

2: 79 percent / 3-methyl-2-selenoxobenzothiazole, trifluoroacetic acid / CH₂Cl₂ / 20 h / Ambient temperature

With N-methyl-1,3-benzothiazole-2(3H)-selone; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)88052-0

Reference yield:

: 75348-12-8
1L-2,3,4-Tri-O-benzyl-1-C-hydroxymethyl-chiro-inositol

: 81713-03-3
2L-(2,3,5/4,6)-4,5,6-Tri-O-benzyl-1-C-methylen-3-O-p-tolylsulfonyl-chiro-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / 12 h / 60 °C

2: 96 percent / sodium methoxide / methanol / 0.75 h / Ambient temperature

3: 79 percent / 3-methyl-2-selenoxobenzothiazole, trifluoroacetic acid / CH₂Cl₂ / 20 h / Ambient temperature

With pyridine; N-methyl-1,3-benzothiazole-2(3H)-selone; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)88052-0