6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one

Base Information

• Chemical Name: 6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one
• CAS No.: 847950-98-5
• Molecular Formula: C₂₁H₁₇N₅O₃S
• Molecular Weight: 419.464

Synonyms:6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one

Chemical Property of 6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one

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Technology Process of 6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one

There total 1 articles about 6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

6-(2,6-dimethylphenyl)-2-methylthiobenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one (847950-97-4) → 6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one (847950-98-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 15h;

DOI:10.1021/jm701095m

Reference yield: 93.0%

6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one (847950-98-5) + N,N-dimethyl-3-(4-aminophenoxy)propylamine (62424-88-8) → 6-(2,6-dimethylphenyl)-2-[4-(3-dimethylaminopropoxy)phenylamino]-benzo[4,5]imidazolo[1,2-a]pyrimido[5,4-e]pyrimidin-5-one

Guidance literature:

With trifluoroacetic acid; In isopropyl alcohol; at 85 ℃; for 15h;

DOI:10.1021/jm701095m

Reference yield: 58.0%

6-(2,6-dimethylphenyl)-2-methanesulfonylbenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one (847950-98-5) + 4-(4-Methyl-piperazino)-anilin (16153-81-4) → 6-(2,6-dimethylphenyl)-2-[4-(4-methylpiperazino)phenylamino]-benzo[4,5]-imidazolo[1,2-a]pyrimido[5,4-e]pyrimidin-5-one (847950-09-8)

Guidance literature:

In isopropyl alcohol; at 85 ℃; for 15h;

DOI:10.1021/jm701095m

upstream raw materials:

6-(2,6-dimethylphenyl)-2-methylthiobenzo[4,5]imidazolo[1,2-a]pyrimido[5,6-e]pyrimidin-5-one

Downstream raw materials:

6-(2,6-dimethylphenyl)-2-[4-(4-methylpiperazino)phenylamino]-benzo[4,5]-imidazolo[1,2-a]pyrimido[5,4-e]pyrimidin-5-one

C₃₆H₄₀N₈O₄

C₃₄H₃₆N₈O₃

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