4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

Base Information

Chemical Name:4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid
CAS No.:131524-50-0
Molecular Formula:C₂₉H₂₂Cl₂O₈
Molecular Weight:569.395
Hs Code.:

Synonyms:4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

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Chemical Property of 4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

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Technology Process of 4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

There total 1 articles about 4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131524-48-6
benzyl 4-(4'-benzyloxy-3'-chloro-6'-hydroxy-2'-methoxybenzoyloxy)-3-chloro-2,6-dihydroxybenzoate

: 131524-50-0
4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; for 2h; Ambient temperature;
DOI:10.1071/CH9901745

Reference yield: 87.0%

: 131524-50-0
4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

: 131524-52-2
benzyl 6-benzyloxy-4,7-dichloro-1,3-dihydroxy-8-methyl-9-oxo-9H-xanthen-2-carboxylate

Guidance literature:: With trifluoroacetic anhydride; In toluene; 1.) 0 deg C, 10 min, 2.) RT, 22 h;
DOI:10.1071/CH9901745

Reference yield:

: 131524-50-0
4-benzyloxy-2-(4'-benzyloxycarbonyl-2'-chloro-3',5'-dihydroxyphenoxy)-5-chloro-6-methylbenzoic acid

: 131524-55-5
6-benzyloxy-4,7-dichloro-1,3-dihydroxy-8-methyl-9H-xanthen-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / trifluoroacetic anhydride / toluene / 1.) 0 deg C, 10 min, 2.) RT, 22 h

2: 92 percent / KOH / dimethylsulfoxide; H₂O / 1.5 h / 120 - 135 °C

With potassium hydroxide; trifluoroacetic anhydride; In water; dimethyl sulfoxide; toluene;
DOI:10.1071/CH9901745