tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate

Base Information

Chemical Name:tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate
CAS No.:1436430-39-5
Molecular Formula:C₂₇H₃₂N₂O₁₀
Molecular Weight:544.558
Hs Code.:

Synonyms:tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate

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Chemical Property of tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate

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Technology Process of tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate

There total 1 articles about tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5256-74-6
1,3-diethyl 2-diazopropanedioate

: 259541-89-4
4-pyrimidin-2-ylbenzoic acid ethyl ester

: 1436430-39-5
tetraethyl 2,2′-(5-(ethoxycarbonyl)-2-(pyrimidin-2-yl)-1,3-phenylene)dimalonate

Guidance literature:: 4-pyrimidin-2-ylbenzoic acid ethyl ester; With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In ethanol; at 20 ℃; for 1h; Schlenk technique; Inert atmosphere;

1,3-diethyl 2-diazopropanedioate; In ethanol; at 75 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1021/jo400572h