α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

Base Information

Chemical Name:α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid
CAS No.:111648-87-4
Molecular Formula:C₂₇H₂₉NO₅
Molecular Weight:447.531
Hs Code.:

Synonyms:α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

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Chemical Property of α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

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Technology Process of α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

There total 10 articles about α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 111648-86-3
benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

: 111648-87-4
α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

Guidance literature:: With sodium hydroxide; In methanol; dichloromethane; for 3h;

Reference yield:

methanolic NaOH: methanolic NaOH

: 111648-86-3
benzyl 4-<<2,6-dimethyl-4-(phenylmethoxy)phenyl>-methyl>-4-methyl-5-oxo-2-phenyl-3-oxazolidinecarboxylate

: 111648-87-4
α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

Guidance literature:: In dichloromethane;

Reference yield:

: 100-52-7
benzaldehyde

: 111648-87-4
α,2,6-trimethyl-4-(phenylmethoxy)-α-<<(phenylmethoxy)carbonyl>amino>benzenepropionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / p-toluenesulfonic acid monohydrate / 1,1,1-trichloro-ethane / 16 h / Heating

2: 1.) potassium hexamethyldisilazane / 1.) toluene, DMF, a) 30 min, b) RT, 30 min, 2.) toluene, DMF, RT, 3 h

3: 74 percent / methanolic NaOH / CH₂Cl₂; methanol / 3 h

With sodium hydroxide; potassium hexamethyldisilazane; toluene-4-sulfonic acid; In methanol; dichloromethane; 1,1,1-trichloroethane;