Technology Process of C20H21(18)FO2
There total 3 articles about C20H21(18)FO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA;
In
acetonitrile;
at 110 ℃;
for 0.5h;
Automated synthesizer;
DOI:10.1016/j.jfluchem.2012.04.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1: titanium tetrachloride; zinc / tetrahydrofuran
2: potassium carbonate / acetone / 3 h / 50 °C / Inert atmosphere
3: potassium carbonate; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA / acetonitrile / 0.5 h / 110 °C / Automated synthesizer
With
titanium tetrachloride; potassium carbonate; [2.2.2]cryptande; zinc; [18F]fluoride ion, cyclotron produced, NCA;
In
tetrahydrofuran; acetone; acetonitrile;
1: McMurry reaction;
DOI:10.1016/j.jfluchem.2012.04.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1: titanium tetrachloride; zinc / tetrahydrofuran
2: potassium carbonate / acetone / 3 h / 50 °C / Inert atmosphere
3: potassium carbonate; [2.2.2]cryptande; [18F]fluoride ion, cyclotron produced, NCA / acetonitrile / 0.5 h / 110 °C / Automated synthesizer
With
titanium tetrachloride; potassium carbonate; [2.2.2]cryptande; zinc; [18F]fluoride ion, cyclotron produced, NCA;
In
tetrahydrofuran; acetone; acetonitrile;
1: McMurry reaction;
DOI:10.1016/j.jfluchem.2012.04.005