alpha-Pyrufuran

Base Information

Chemical Name:alpha-Pyrufuran
CAS No.:88256-05-7
Molecular Formula:C₁₅H₁₄O₅
Molecular Weight:274.273
Hs Code.:
UNII:TKD25ZL66T
DSSTox Substance ID:DTXSID40236927
Nikkaji Number:J591.333K
Wikidata:Q27108617
Metabolomics Workbench ID:44482

Synonyms:alpha-Pyrufuran;1,3,4-Trimethoxydibenzofuran-2-ol;2-Dibenzofuranol, 1,3,4-trimethoxy-;88256-05-7;1,3,4-Trimethoxy-2-dibenzofuranol;a-Pyrufuran;.alpha.-Pyrufuran;C08929;TKD25ZL66T;CHEBI:10328;DTXSID40236927;1,3,4-Trimethoxy-2-dibenzofuranol, 9CI;1,3,4-Trimethoxydibenzo[b,d]furan-2-ol #;Q27108617;3,5,6-trimethoxy-8-oxatricyclo[7.4.0.0^{2,7}]trideca-1(13),2,4,6,9,11-hexaen-4-ol

Suppliers and Price of alpha-Pyrufuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of alpha-Pyrufuran

Chemical Property:

Vapor Pressure:1.77E-08mmHg at 25°C
Boiling Point:443.5°C at 760 mmHg
Flash Point:222°C
Density:1.3g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:274.08412354
Heavy Atom Count:20
Complexity:336

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C2=C1C3=CC=CC=C3O2)OC)OC)O

Technology Process of alpha-Pyrufuran

There total 10 articles about alpha-Pyrufuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 93973-17-2
2-mesyloxy-1,3,4-trimethoxydibenzofuran

: 88256-05-7
1,3,4-trimethoxydibenzofuran-2-ol

Guidance literature:: With sodium hydroxide; water; In 1,4-dioxane; for 1h; Heating;

Reference yield: 5.0%

: 88256-10-4
1,3,4-trimethoxydibenzofuran

: 88256-05-7
1,3,4-trimethoxydibenzofuran-2-ol

Guidance literature:: With n-butyllithium; lithium tert-butyl hydroperoxide; 1.) hexane, Et2O, 4 deg C, 48 h, 2.) -78 deg C -> RT, then reflux, 5 min;

Reference yield:

: 93973-18-3
γ-pyrufuran

: 88256-05-7
1,3,4-trimethoxydibenzofuran-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / pyridine / 0.5 h / 80 °C

2: 50 percent / hydrogen, triethylamine / palladium on charcoal / 2 h / Heating

3: 96 percent / sodium hydroxide, water / dioxane / 1 h / Heating

With pyridine; sodium hydroxide; water; hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane;