(S)-3-(benzyloxy)-1-<methyl>propanol

Base Information

Chemical Name:(S)-3-(benzyloxy)-1-<methyl>propanol
CAS No.:127517-82-2
Molecular Formula:C₃₁H₃₂O₄
Molecular Weight:468.593
Hs Code.:

(S)-3-(benzyloxy)-1-<<diphenyl(4-methoxyphenyl)methoxy>methyl>propanol

Synonyms:(S)-3-(benzyloxy)-1-<methyl>propanol

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Chemical Property of (S)-3-(benzyloxy)-1-<methyl>propanol

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Technology Process of (S)-3-(benzyloxy)-1-<methyl>propanol

There total 6 articles about (S)-3-(benzyloxy)-1-<methyl>propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (S)-4-O-benzyl-1,2,4-butanetriol

: 14470-28-1
mono-4-methoxytrityl chloride

: 127517-82-2
(S)-3-(benzyloxy)-1-<methyl>propanol

Guidance literature:: With 2-(Dimethylamino)pyridine; sodium hydrogencarbonate; triethylamine; In dichloromethane;

Reference yield: 95.0%

: 71998-69-1,86990-91-2,104973-80-0,69985-32-6
(S)-4-benzyloxy-1,2-butanediol

: 14470-28-1
mono-4-methoxytrityl chloride

: 127517-82-2
(S)-3-(benzyloxy)-1-<methyl>propanol

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 5.5h;
DOI:10.1021/jm00071a003

Reference yield:

: 100-39-0
benzyl bromide

: 127517-82-2
(S)-3-(benzyloxy)-1-<methyl>propanol

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammonium iodide, conc. aq. NaOH / 18 h / 110 °C

2: 1.5 M aq. H₂SO₄ / 8 h / 100 °C

3: 95 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 5.5 h / 0 - 20 °C

With dmap; sodium hydroxide; sulfuric acid; tetra-(n-butyl)ammonium iodide; triethylamine; In dichloromethane;
DOI:10.1021/jm00071a003