[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4

Base Information

• Chemical Name: [CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4
• CAS No.: 754227-22-0
• Molecular Formula: C₂₃H₂₆NOPRe*C₂₄H₂₀B
• Molecular Weight: 868.88

Synonyms:[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4

Chemical Property of [CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4

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Technology Process of [CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4

There total 1 articles about [CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[CH₃Re(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[HRe(CO)(C5H4C2H4N(CH3)CH2P(C6H5)2)](1+)*B(C6H5)4(1-)=[HRe(CO)(C5H4C2H4N(CH3)CH2P(C6H5)2)]B(C6H5)4 (754227-14-0) + methyl iodide (74-88-4) → [CH3Re(CO)(C5H4C2H4N(CH3)CH2P(C6H5)2)](1+)*B(C6H5)4(1-)=[CH3Re(CO)(C5H4C2H4N(CH3)CH2P(C6H5)2)]B(C6H5)4 (754227-22-0)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; a soln. of Li compd. (1.2 equiv., hexane) added (0°C, 1 min) to asuspn. of Re compd. (THF), stirred for 20 min, CH3I added, stirred at r oom. temp. for 1 h; concd. (vac.), washed (methanol, diethyl ether), recrystd. (acetone/hexane); elem. anal.;

DOI:10.1002/ejic.200300650

upstream raw materials:

[HRe(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[HRe(CO)(C₅H₄C₂H₄N(CH₃)CH₂P(C₆H₅)2)]B(C₆H₅)4

methyl iodide

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