cyclohexyl 2-oxopropanoate

Base Information

• Chemical Name: cyclohexyl 2-oxopropanoate
• CAS No.: 6963-43-5
• Molecular Formula: C9H14O3
• Molecular Weight: 170.2057
• Mol file: 6963-43-5.mol

Synonyms:

Chemical Property of cyclohexyl 2-oxopropanoate

Chemical Property:

• Vapor Pressure: 0.0246mmHg at 25°C
• Boiling Point: 248.2°Cat760mmHg
• Flash Point: 104°C
• Density: 1.06g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of cyclohexyl 2-oxopropanoate

There total 2 articles about cyclohexyl 2-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

cyclohexyl acrylate (3066-71-5,27458-65-7) → c-hexyl pyruvate (6963-43-5) + cyclohexyl 2-hydroxypropanoate (68791-95-7) + 2-Hydroperoxy-propionic acid cyclohexyl ester (143713-49-9)

Guidance literature:

With triethylsilane; porphyrin‐Co(II); oxygen; In dichloromethane; isopropyl alcohol; for 3h; Ambient temperature;

DOI:10.1246/cl.1992.1381

Reference yield:

cyclohexyl acrylate (3066-71-5,27458-65-7) → c-hexyl pyruvate (6963-43-5)

Guidance literature:

With triethylsilane; dmap; porphyrin‐Co(II); oxygen; acetic anhydride; Yield given. Multistep reaction; 1.) isopropanol, CH₂Cl₂, RT, 3 h, 2.) CH₂Cl₂, RT, 6 h;

DOI:10.1246/cl.1992.1381

Reference yield:

c-hexyl pyruvate (6963-43-5) → N-cyclohexyl-L-alanine (82017-30-9) + N-cyclohexyl-D-alanine

Guidance literature:

With D-Glucose; ammonium chloride; glucose dehydrogenase; at 20 ℃; for 6h; pH=9.0; Sodium carbonate/bicarbonate buffer;

upstream raw materials:

cyclohexyl acrylate

Downstream raw materials:

N-cyclohexyl-L-alanine