N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate

Base Information

• Chemical Name: N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate
• CAS No.: 125972-09-0
• Molecular Formula: C₈H₅Cl₃F₃N₂OP
• Molecular Weight: 339.468
• Mol file: 125972-09-0.mol

Synonyms:N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate

Chemical Property of N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate

There total 2 articles about N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ5-oxadiazaphospholine (86508-62-5) → N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate (125972-09-0)

Guidance literature:

With hydrogenchloride; In tetrachloromethane; for 2h; Heating;

Reference yield:

2,2,2-trifluoro-N′-phenylacetohydrazide (34064-31-8) → N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate (125972-09-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / PCl₅, POCl₃ / 2 h

2: 90 percent / HCl / CCl₄ / 2 h / Heating

With hydrogenchloride; phosphorus pentachloride; trichlorophosphate; In tetrachloromethane;

Reference yield:

N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate (125972-09-0) → 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ5-oxadiazaphospholine (86508-62-5)

Guidance literature:

Heating; distillation;

upstream raw materials:

2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine

2,2,2-trifluoro-N′-phenylacetohydrazide

Downstream raw materials:

2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine