25-benzyloxy-26,27,28-trihydroxycalix<4>arene

Base Information

Chemical Name:25-benzyloxy-26,27,28-trihydroxycalix<4>arene
CAS No.:134225-80-2
Molecular Formula:C₃₅H₃₀O₄
Molecular Weight:514.621
Hs Code.:

Synonyms:25-benzyloxy-26,27,28-trihydroxycalix<4>arene

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Chemical Property of 25-benzyloxy-26,27,28-trihydroxycalix<4>arene

Chemical Property:

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Technology Process of 25-benzyloxy-26,27,28-trihydroxycalix<4>arene

There total 4 articles about 25-benzyloxy-26,27,28-trihydroxycalix<4>arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 248590-47-8,74568-07-3
25,26,27,28-tetrakis(hydroxy)calix[4]arene

: 100-39-0
benzyl bromide

: 134225-80-2
25-benzyloxy-26,27,28-trihydroxycalix<4>arene

Guidance literature:: With sodium methylate; In acetonitrile; for 9h; Heating;
DOI:10.1021/jo981648l

Reference yield:

: 248590-47-8,74568-07-3
25,26,27,28-tetrakis(hydroxy)calix[4]arene

: 134225-80-2
25-benzyloxy-26,27,28-trihydroxycalix<4>arene

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 24 h / Heating

2: Me₃SiI / CHCl₃ / 3 h / Ambient temperature

With trimethylsilyl iodide; potassium carbonate; In chloroform; acetonitrile;
DOI:10.1016/S0040-4020(01)96132-0