2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Base Information

Chemical Name:2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide
CAS No.:1437872-76-8
Molecular Formula:C₄₄H₃₇N₅O₁₁
Molecular Weight:811.805
Hs Code.:

Synonyms:2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

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Chemical Property of 2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

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Technology Process of 2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

There total 19 articles about 2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1437872-89-3
2-(benzyloxy)-3-(3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenyl)benzamide

: 1437872-76-8
2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Guidance literature:: With palladium on activated charcoal; hydrogen; In tetrahydrofuran; methanol; at 40 ℃; for 3h;
DOI:10.1039/c3cc42349b

Reference yield:

: 22621-41-6
2-hydroxy-3-nitro-benzoic acid methyl ester

: 1437872-76-8
2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C

2.1: sodium hydroxide / methanol; water / 2 h / Reflux

2.2: pH 1

3.1: thionyl chloride / 2 h / Reflux

4.1: iron; acetic acid / ethanol / 2 h / Reflux

5.1: thionyl chloride / 2 h / Reflux

6.1: iron; acetic acid / ethanol / 2 h / Reflux

7.1: thionyl chloride / 2 h / Reflux

8.1: iron; acetic acid / ethanol / 2 h / Reflux

9.1: thionyl chloride / 2 h / Reflux

10.1: hydrogen; palladium on activated charcoal / tetrahydrofuran; methanol / 3 h / 40 °C

With thionyl chloride; palladium on activated charcoal; hydrogen; iron; potassium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42349b

Reference yield:

: 90564-26-4
2-methoxy-3-nitro-benzoic acid methyl ester

: 1437872-76-8
2-hydroxy-3-(3-(2-hydroxy-3-(2-methoxybenzamido)benzamido)-2-methoxybenzamido)-N-(3-(2-hydroxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / methanol; water / 2 h / Reflux

1.2: pH 1

2.1: thionyl chloride / 2 h / Reflux

3.1: iron; acetic acid / ethanol / 2 h / Reflux

4.1: thionyl chloride / 2 h / Reflux

5.1: hydrogen; palladium on activated charcoal / tetrahydrofuran; methanol / 3 h / 40 °C

With thionyl chloride; palladium on activated charcoal; hydrogen; iron; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1039/c3cc42349b