(C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl

Base Information

Chemical Name:(C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl
CAS No.:92078-41-6
Molecular Formula:C₅₆H₄₂ClFeN₁₀O₄
Molecular Weight:1010.31
Hs Code.:

(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>5</sub>)2(C<sub>6</sub>H<sub>4</sub>NHCOOCH<sub>2</sub>CH<sub>2</sub>C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>)2)FeCl

Synonyms:(C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl

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Chemical Property of (C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl

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Technology Process of (C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl

There total 1 articles about (C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-44-5
phosgene

: 1615-14-1
1-(2-Hydroxyethyl)imidazole

: (C₂₀H₈N₄(C₆H₅)2(C₆H₄NH₂)2)FeCl

: 92078-41-6
(C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl

Guidance literature:: With pyridine; In dichloromethane; benzene; a soln. of Fe-complex in CH2Cl2-Py (4:1 v/v) was added slowly dropwise to a soln. of COCl2 in benzene-CH2Cl2 with stirring, once the addn. was complete a soln. of ImCH2CH2OH in CH2Cl2 was added dropwise, the mixt. was stirred overnight; reaction mixt. was extd. 6 times with water at pH 5.0, placed on a dry SiO2 column and eluted with 10% MeOH in CHCl3;
DOI:10.1021/ja00335a003

Reference yield:

: 92078-41-6
(C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₃N₂)2)FeCl

: (C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₄N₂)2)FeCl⁽²⁺⁾*2Cl^(1-)=((C₂₀H₈N₄(C₆H₅)2(C₆H₄NHCOOCH₂CH₂C₃H₄N₂)2)FeCl)Cl₂

Guidance literature:: With hydrogenchloride; In dichloromethane; Fe-complex was treated with HCl gas in dry CH2Cl2; evapd. to dryness;
DOI:10.1021/ja00335a003