Technology Process of 4-[(4-hexylphenyl)diazenyl]phenol
There total 7 articles about 4-[(4-hexylphenyl)diazenyl]phenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-hexylaniline;
With
hydrogenchloride; sodium nitrite;
In
water; acetone;
at 2 ℃;
for 0.333333h;
Cooling with ice;
phenol;
With
sodium carbonate; sodium hydroxide;
In
water; acetone;
at 8 ℃;
Cooling with ice;
DOI:10.1039/c9tc04079j
- Guidance literature:
-
4-hexylaniline;
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 - 5 ℃;
Inert atmosphere;
phenol;
With
sodium hydroxide;
In
water;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrazine
2.1: aluminum (III) chloride; acetyl chloride
3.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C
3.2: 1 h / 0 °C
With
hydrogenchloride; aluminum (III) chloride; acetyl chloride; hydrazine; sodium nitrite;
In
water;
2.2: Schmidt reaction;
DOI:10.1080/15421400903065754
