N₁-(4-Methoxybenzoyl)-N₂-[4-(methylthio)benzoyl]-1,2-benzenediamine

Base Information

• Chemical Name: N₁-(4-Methoxybenzoyl)-N₂-[4-(methylthio)benzoyl]-1,2-benzenediamine
• CAS No.: 219489-93-7
• Molecular Formula: C₂₂H₂₀N₂O₃S
• Molecular Weight: 392.478
• Mol file: 219489-93-7.mol

Synonyms:N₁-(4-Methoxybenzoyl)-N₂-[4-(methylthio)benzoyl]-1,2-benzenediamine

Chemical Property of N₁-(4-Methoxybenzoyl)-N₂-[4-(methylthio)benzoyl]-1,2-benzenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₁-(4-Methoxybenzoyl)-N₂-[4-(methylthio)benzoyl]-1,2-benzenediamine

There total 3 articles about N₁-(4-Methoxybenzoyl)-N₂-[4-(methylthio)benzoyl]-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(methylthio)benzoyl chloride (1442-06-4) + N1-(4-methoxybenzoyl)-1,2-benzenediamine (103517-57-3) → N1-(4-Methoxybenzoyl)-N2-[4-(methylthio)benzoyl]-1,2-benzenediamine (219489-93-7)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jm990326m

Reference yield:

4-(methylthio)benzoic acid (13205-48-6,562836-64-0) → N1-(4-Methoxybenzoyl)-N2-[4-(methylthio)benzoyl]-1,2-benzenediamine (219489-93-7)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂; pyridine / toluene / 3 h / 80 °C

2: pyridine / CH₂Cl₂ / 1 h / 20 °C

With pyridine; thionyl chloride; In dichloromethane; toluene; 1: Chlorination / 2: Acylation;

DOI:10.1021/jm990326m

Reference yield:

→ N1-(4-Methoxybenzoyl)-N2-[4-(methylthio)benzoyl]-1,2-benzenediamine (219489-93-7)

Guidance literature:

upstream raw materials:

4-(methylthio)benzoyl chloride

N₁-(4-methoxybenzoyl)-1,2-benzenediamine

4-(methylthio)benzoic acid