2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

Base Information

Chemical Name:2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal
CAS No.:1332330-03-6
Molecular Formula:C₂₅H₃₅N₃O₇
Molecular Weight:489.569
Hs Code.:

Synonyms:2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

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Chemical Property of 2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

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Technology Process of 2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

There total 5 articles about 2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1332330-01-4
2,5-anhydro-6-O-benzoyl-4-O-decanoyl-3-O-methanesulfonyl-D-glucose ethylene acetal

: 1332330-03-6
2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 110 ℃; for 27h;
DOI:10.1016/j.tet.2011.06.090

Reference yield:

: 1332329-99-3
2,5-anhydro-4-O-n-decanoyl-3,6-di-O-methanesulfonyl-D-glucose ethylene acetal

: 1332330-03-6
2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 12 h / 100 °C

2: sodium azide / dimethyl sulfoxide / 27 h / 110 °C

With sodium azide; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.06.090

Reference yield:

: 157506-35-9
2,5-anhydro-3,6-di-O-methanesulfonyl-D-glucose ethylene acetal

: 1332330-03-6
2,5-anhydro-3-azido-6-O-benzoyl-4-O-decanoyl-3-deoxy-D-allose ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 48.25 h / 0 - 20 °C

2: N,N-dimethyl-formamide / 12 h / 100 °C

3: sodium azide / dimethyl sulfoxide / 27 h / 110 °C

With pyridine; sodium azide; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.06.090