4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Base Information

Chemical Name:4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate
CAS No.:1357362-67-4
Molecular Formula:C₂₀H₁₅NO₇S₃
Molecular Weight:477.54
Hs Code.:

Synonyms:4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Suppliers and Price of 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 18 raw suppliers

Chemical Property of 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Chemical Property:

Boiling Point:671.5±65.0 °C(Predicted)
Density:1.53±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

There total 4 articles about 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2-{[(4-nitroxy)butanoyl]oxy}benzoic acid

: 18274-81-2
desmethyl anethole trithione

: 1357362-67-4
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ml300002m

Reference yield:

: 937808-67-8
2-formylphenyl 4-bromobutanoate

: 1357362-67-4
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: silver nitrate / acetonitrile / 12 h / 20 °C

2: potassium permanganate / acetone / 3 h / 0 - 20 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; potassium permanganate; silver nitrate; dicyclohexyl-carbodiimide; In dichloromethane; acetone; acetonitrile;
DOI:10.1021/ml300002m

Reference yield:

: 90-02-8
salicylaldehyde

: 1357362-67-4
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 2-((4-(nitrooxy)butanoyl)oxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 6 h / 20 °C

2: silver nitrate / acetonitrile / 12 h / 20 °C

3: potassium permanganate / acetone / 3 h / 0 - 20 °C

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; potassium permanganate; silver nitrate; dicyclohexyl-carbodiimide; In dichloromethane; acetone; acetonitrile;
DOI:10.1021/ml300002m