5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

Base Information

Chemical Name:5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole
CAS No.:1355330-15-2
Molecular Formula:C₁₈H₁₇N₅O₈
Molecular Weight:431.362
Hs Code.:

Synonyms:5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

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Chemical Property of 5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

Chemical Property:

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Technology Process of 5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

There total 3 articles about 5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1355330-31-2
1-ethynyl-2,3-dinitro-4-methoxybenzene

: 115483-29-9
3,4,5-trimethoxyphenyl azide

: 1355330-22-1
4-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

: 1355330-15-2
5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

Guidance literature:: In water; toluene; for 72h; Reflux;
DOI:10.1016/j.bmc.2011.11.010

Reference yield:

: 22996-21-0
4-methoxy-2-nitro-benzaldehyde

: 1355330-15-2
5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 0 °C

2: potassium carbonate / methanol / 1.5 h

3: water; toluene / 72 h / Reflux

With sulfuric acid; nitric acid; potassium carbonate; In methanol; water; toluene; 2: Ohira-Bestmann reaction / 3: Huisgen cycloaddition;
DOI:10.1016/j.bmc.2011.11.010

Reference yield:

: 519060-36-7
4-methoxy-2,3-dinitrobenzaldehyde

: 1355330-15-2
5-(4-methoxy-2,3-dinitrophenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 1.5 h

2: water; toluene / 72 h / Reflux

With potassium carbonate; In methanol; water; toluene; 1: Ohira-Bestmann reaction / 2: Huisgen cycloaddition;
DOI:10.1016/j.bmc.2011.11.010