Acetic acid, cyano((4-methylphenyl)hydrazono)-, ethyl ester

Base Information

Chemical Name:Acetic acid, cyano((4-methylphenyl)hydrazono)-, ethyl ester
CAS No.:6797-29-1
Molecular Formula:C12H13N3O2
Molecular Weight:231.254
Hs Code.:

Synonyms:6797-29-1;Cyanoglyoxylic acid ethyl ester 2-p-tolylhydrazone;ACETIC ACID, CYANO((4-METHYLPHENYL)HYDRAZONO)-, ETHYL ESTER;Glyoxylic acid, cyano-, ethyl ester, 2-p-tolylhydrazone;ethyl cyano[(4-methylphenyl)hydrazono]acetate;ethyl (2E)-2-cyano-2-[(4-methylphenyl)hydrazinylidene]acetate;ethyl (2E)-cyano[(4-methylphenyl)hydrazono]acetate;MFCD00853281;AKOS003581615;BS-4362;AE-848/32190049

Suppliers and Price of Acetic acid, cyano((4-methylphenyl)hydrazono)-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, cyano((4-methylphenyl)hydrazono)-, ethyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:338.134°C at 760 mmHg
Flash Point:158.298°C
Density:1.125g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:231.100776666
Heavy Atom Count:17
Complexity:335

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=NNC1=CC=C(C=C1)C)C#N
Isomeric SMILES:CCOC(=O)/C(=N/NC1=CC=C(C=C1)C)/C#N

Technology Process of Acetic acid, cyano((4-methylphenyl)hydrazono)-, ethyl ester

There total 4 articles about Acetic acid, cyano((4-methylphenyl)hydrazono)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 459-44-9
4-methylbenzenediazonium tetrafluoroborate

: 105-56-6
ethyl 2-cyanoacetate

: 6797-29-1
cyano[(4-methylphenyl)hydrazono]acetic acid ethyl ester

Guidance literature:: With sodium acetate; silica gel; In neat (no solvent); at 20 ℃; for 0.333333h; Milling;
DOI:10.2174/1570178611999140404111411

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 105-56-6
ethyl 2-cyanoacetate

: 6797-29-1
cyano[(4-methylphenyl)hydrazono]acetic acid ethyl ester

Guidance literature:: p-toluidine; With hydrogenchloride; sodium nitrite;

ethyl 2-cyanoacetate;
DOI:10.1016/j.molstruc.2016.07.043

Reference yield:

: 2028-84-4
p-methylbenzenediazonium chloride

: 105-56-6
ethyl 2-cyanoacetate

: 6797-29-1
cyano[(4-methylphenyl)hydrazono]acetic acid ethyl ester

Guidance literature:: With ethanol; sodium acetate; β-form; man fuehrt das Reaktionsprodukt durch Behandeln mit alkoh. Kali in ein Kaliumsalz ueber und zerlegt dieses in waessr. Loesung durch Einleiten von Kohlendioxyd;