C₃₂H₂₉BF₂N₄O₂

Base Information

Chemical Name:C₃₂H₂₉BF₂N₄O₂
CAS No.:1301766-13-1
Molecular Formula:C₃₂H₂₉BF₂N₄O₂
Molecular Weight:550.416
Hs Code.:

C<sub>32</sub>H<sub>29</sub>BF<sub>2</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₃₂H₂₉BF₂N₄O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₂₉BF₂N₄O₂

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Technology Process of C₃₂H₂₉BF₂N₄O₂

There total 3 articles about C₃₂H₂₉BF₂N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1301766-12-0
C₂₄H₁₉BBrF₂N₃O₂

: 28611-39-4
4-(dimethylamino)benzene-boronic acid

: 1301766-13-1
C₃₂H₂₉BF₂N₄O₂

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; water; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol200799u

Reference yield:

: 870753-29-0
8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

: 1301766-13-1
C₃₂H₂₉BF₂N₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

2: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; XPhos / 1,4-dioxane; water / 48 h / 20 °C / Inert atmosphere

3: N-Bromosuccinimide / dichloromethane; N,N-dimethyl-formamide / 1.5 h / 20 °C

4: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; XPhos; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 2: Suzuki coupling / 4: Suzuki coupling;
DOI:10.1021/ol200799u

Reference yield:

: 1301766-05-1
C₁₈H₁₆BBrF₂N₂

: 1301766-13-1
C₃₂H₂₉BF₂N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; XPhos / 1,4-dioxane; water / 48 h / 20 °C / Inert atmosphere

2: N-Bromosuccinimide / dichloromethane; N,N-dimethyl-formamide / 1.5 h / 20 °C

3: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate / tetrahydrofuran; water / 24 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; XPhos; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 1: Suzuki coupling / 3: Suzuki coupling;
DOI:10.1021/ol200799u