S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

Base Information

Chemical Name:S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate
CAS No.:1246016-72-7
Molecular Formula:C₂₂H₂₄F₂O₄S₂
Molecular Weight:454.559
Hs Code.:

Synonyms:S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

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Chemical Property of S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

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Technology Process of S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

There total 1 articles about S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 19754-21-3
1-allyl-2,3-dimethoxy-benzene

: dithiocarbonic acid S-[2-(2,4-difluoro-phenyl)-2-oxo-ethyl] ester O-ethyl ester

: 1246016-72-7
S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2010.06.006

Reference yield: 92.0%

: 1246016-72-7
S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

: 1246017-03-7
2-(2,3-dimethoxybenzyl)-7-fluoro-2,3-dihydro-thieno[2,3-b]thiochromen-4-one

Guidance literature:: With potassium carbonate; In acetonitrile; tert-butyl alcohol; for 3.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2010.06.006

Reference yield: 82.0%

: 1246016-72-7
S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate

: 1246016-82-9
2-(2,3-dimethoxybenzyl)-8-fluoro-3,4-dihydro-2H-benzo[b]thiepin-5-one

Guidance literature:: S-(5-(2,4-difluorophenyl)-1-(2,3-dimethoxyphenyl)-5-oxopentan-2-yl) O-ethyl carbonodithioate; With ethylenediamine; In diethyl ether; ethanol; at 20 ℃; for 0.333333h; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; Inert atmosphere; Reflux;
DOI:10.1016/j.tetasy.2010.06.006