2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

Base Information

Chemical Name:2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione
CAS No.:1570084-70-6
Molecular Formula:C₁₈H₁₅N₃O₃S
Molecular Weight:353.401
Hs Code.:

Synonyms:2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

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Chemical Property of 2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

Chemical Property:

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Technology Process of 2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

There total 7 articles about 2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1570084-42-2
2-[[4-(methylsulfonimidoyl)phenyl]methyl]isoindoline-1,3-dione

: 590-17-0
cyanomethyl bromide

: 1570084-70-6
2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

Guidance literature:: 2-[[4-(methylsulfonimidoyl)phenyl]methyl]isoindoline-1,3-dione; With potassium hydride; In 1,2-dimethoxyethane; at 20 ℃; for 0.25h;

cyanomethyl bromide; With tetraethylammonium bromide; In 1,2-dimethoxyethane; at 110 ℃;

Reference yield:

: 1570084-40-0
N-[[4-[(1,3-dioxoisoindolin-2-yl)methyl]phenyl]-methyl-oxo-λ⁶-sulfanylidene]-2,2,2-trifluoro-acetamide

: 1570084-70-6
2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / methanol / 16 h / 20 °C

2.1: potassium hydride / 1,2-dimethoxyethane / 0.25 h / 20 °C

2.2: 110 °C

With potassium hydride; potassium carbonate; In methanol; 1,2-dimethoxyethane;

Reference yield:

: 85-44-9
phthalic anhydride

: 1570084-70-6
2-(4-(N-cyanomethyl-S-(methyl)sulfonimidoyl)benzyl)isoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / 3 h / Reflux

2.1: N-Bromosuccinimide; potassium tert-butylate / methanol / 1 h

3.1: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / ethanol / 0 - 20 °C

4.1: dichloromethane / 2 h / 0 - 20 °C

5.1: potassium carbonate / methanol / 16 h / 20 °C

6.1: potassium hydride / 1,2-dimethoxyethane / 0.25 h / 20 °C

6.2: 110 °C

With N-Bromosuccinimide; potassium tert-butylate; potassium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; acetic acid;