η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate

Base Information

Chemical Name:η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate
CAS No.:221639-17-4
Molecular Formula:C₂₀H₂₂FeNSe*F₆P
Molecular Weight:556.173
Hs Code.:

Synonyms:η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate

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Chemical Property of η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate

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Technology Process of η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate

There total 1 articles about η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 2-methylchlorobenzene-eta.5-cyclopentadienyliron hexafluorophosphate

: 52673-28-6
4,4′(N,N′-dimethylaniline)diselenide

: 221639-17-4
η(6)-[4-(dimethylamino)phenylseleno]-2-methylbenzene-η(5)-(cyclopentadienyl)iron hexafluorophosphate

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; acetone; Ph2Se2 soln. (THF) dropwise addn. to NaBH4 soln. (EtOH), Fe-compd. suspn. (Me2CO) addn., stirring (room temp., overnight), evapn., 0.1 M HCl / NH4PF4 addn., NaHCO3 addn.; extg. (CH2Cl2), drying, evapn., chromy. (alumina, ether, Me2CO), crystn.(Me2CO / ether); elem. anal.;
DOI:10.1021/om980948q