N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

Base Information

Chemical Name:N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide
CAS No.:1227850-86-3
Molecular Formula:C₂₃H₂₃N₃O₅S
Molecular Weight:453.519
Hs Code.:

Synonyms:N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

Suppliers and Price of N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

There total 1 articles about N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2002-03-1
2-amino-5-phenyl-1,3,4-thiadiazole

: 1227850-52-3
(1H-benzo[d][1,2,3]triazol-1-yl)(6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanone

: 1227850-86-3
N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.2174/157017810790796363

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 1227850-86-3
N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

: C₂₉H₂₆N₆O₄S

Guidance literature:: N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide; With pyridine; oxalyl dichloride; In dichloromethane; at 0 ℃; for 0.25h;

1,2,3-Benzotriazole; In dichloromethane; at 0 - 40 ℃; for 7.25h;
DOI:10.1080/07328303.2011.652790

Reference yield:

: 1227850-86-3
N-(5-phenyl[1,3,4]thiadiazol-2-yl)-3-O-benzyl-1,2-O-isopropylidene-α-D-xylo-furanuronamide

: 1361329-06-7
C₂₃H₂₂N₆O₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; oxalyl dichloride / dichloromethane / 0.25 h / 0 °C

1.2: 7.25 h / 0 - 40 °C

2.1: sodium azide / N,N-dimethyl-formamide / 10 h / 50 °C

With pyridine; sodium azide; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328303.2011.652790