2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

Base Information

Chemical Name:2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene
CAS No.:1416136-86-1
Molecular Formula:C₄₁H₄₈N₂O₅
Molecular Weight:648.843
Hs Code.:

Synonyms:2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

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Chemical Property of 2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

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Technology Process of 2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

There total 3 articles about 2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1416136-82-7
2-[3-(benzyloxy)phenyl]-1,1-bis(4-hydroxyphenyl)-1-butene

: 3647-69-6
4-(2-chloroethyl)morpholine hydrochride

: 1416136-86-1
2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

Guidance literature:: 2-[3-(benzyloxy)phenyl]-1,1-bis(4-hydroxyphenyl)-1-butene; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.25h; Inert atmosphere;

4-(2-chloroethyl)morpholine hydrochride; With ammonium chloride; In N,N-dimethyl-formamide; at 50 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.10.037

Reference yield:

: 611-99-4
4,4'-Dihydroxybenzophenone

: 1416136-86-1
2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc; titanium tetrachloride; potassium carbonate / tetrahydrofuran / 2 h / 0 - 90 °C / Darkness; Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 - 20 °C / Inert atmosphere

2.2: 6 h / 50 °C / Inert atmosphere

With titanium tetrachloride; sodium hydride; potassium carbonate; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.10.037

Reference yield:

: 37951-47-6
3-benzyloxyphenyl ethyl ketone

: 1416136-86-1
2-[3-(benzyloxy)phenyl]-1,1-bis{4-[2-(morpholin-4-yl)ethoxy]phenyl}-1-butene

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc; titanium tetrachloride / tetrahydrofuran / 2 h / 0 - 90 °C / Darkness

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 - 20 °C

2.2: 6 h / 50 °C

With titanium tetrachloride; sodium hydride; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;