L-proline phenacyl ester

Base Information

Chemical Name:L-proline phenacyl ester
CAS No.:87016-40-8
Molecular Formula:C₁₃H₁₅NO₃
Molecular Weight:233.267
Hs Code.:

Synonyms:L-proline phenacyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of L-proline phenacyl ester

Chemical Property:

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Technology Process of L-proline phenacyl ester

There total 2 articles about L-proline phenacyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16153-10-9
N<(benzyloxy)carbonyl>-L-proline phenacyl ester

: 87016-40-8
L-proline phenacyl ester

Guidance literature:: With hydrogen bromide; In acetic acid; ethyl acetate;
DOI:10.1021/ja00299a038

Reference yield:

: 110345-80-7
1-(tert-butyl) 2-(2-oxo-2-phenylethyl) (S)-pyrrolidine-1,2-dicarboxylate

: 87016-40-8
L-proline phenacyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / ethyl acetate / 3 h

2: N-methylmorpholine

With 4-methyl-morpholine; hydrogenchloride; In ethyl acetate;
DOI:10.1246/bcsj.59.2433

Reference yield:

: 87016-40-8
L-proline phenacyl ester

: H-Gly-Gly-Pro-Gly-Ala-Gly-OPac hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: dicyclohexylcarbodiimide / 3 h, 0 deg C; RT overnight

2: AcOH / Zn / Ambient temperature

3: dicyclohexylcarbodiimide / 3 h, 0 deg C; RT overnight

4: AcOH / Zn / Ambient temperature

5: dicyclohexylcarbodiimide / 3 h, 0 deg C; RT overnight

6: AcOH / Zn / Ambient temperature

7: dicyclohexylcarbodiimide / 3 h, 0 deg C; RT overnight

8: aq. HCl / ethyl acetate / 1.5 h

With hydrogenchloride; acetic acid; dicyclohexyl-carbodiimide; zinc; In ethyl acetate;
DOI:10.1246/bcsj.59.2433