bis(2,6-diisopropylphenyl)glyoxal

Base Information

• Chemical Name: bis(2,6-diisopropylphenyl)glyoxal
• CAS No.: 960049-71-2
• Molecular Formula: C₂₆H₃₄O₂
• Molecular Weight: 378.555

Synonyms:bis(2,6-diisopropylphenyl)glyoxal

Chemical Property of bis(2,6-diisopropylphenyl)glyoxal

Chemical Property:

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Technology Process of bis(2,6-diisopropylphenyl)glyoxal

There total 1 articles about bis(2,6-diisopropylphenyl)glyoxal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2C4H10O*2C12H17Li + carbon monoxide (201230-82-2) → bis(2,6-diisopropylphenyl)glyoxal (960049-71-2)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1039/b713062g

Reference yield: 63.0%

bis(2,6-diisopropylphenyl)glyoxal (960049-71-2) + diethyl ether (60-29-7,927820-24-4) + cobalt(II) chloride (7646-79-9,14543-09-0,16413-89-1) → [Co(II)(bis(2,6-diisopropylphenyl)glyoxal(1-))2(diethyl ether)]

Guidance literature:

With sodium; In diethyl ether; under Ar; CoCl2 and Na added to soln. of ligand (molar ratio 1:2:2) in Et2O at 20°C with stirring; stirred for 48 h; solvent removed in vac.; extd. in Et2O; filtered; crystd. by slow evapn.; elem. anal.;

DOI:10.1021/ic801470p

Reference yield: 62.0%

chromium dichloride + bis(2,6-diisopropylphenyl)glyoxal (960049-71-2) → [Cr((COC6H3(CH(CH3)2)2)2)3]

Guidance literature:

With sodium; In diethyl ether; under inert atm.; soln. of bis(2,6-diisopropylphenyl)glyoxal in Et2O added to CrCl2 and Na under stirring, mixt. stirred for 24 h; evapd. under vac., residue extd. with Et2O, soln. filtered, filtrate allowed to evap. slowly; elem. anal.;

DOI:10.1021/ic801122m

upstream raw materials:

carbon monoxide

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