2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Base Information

Chemical Name:2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid
CAS No.:119784-79-1
Molecular Formula:C₂₅H₃₄N₄O₄
Molecular Weight:454.569
Hs Code.:

Synonyms:2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Suppliers and Price of 2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

There total 7 articles about 2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 541-41-3
chloroformic acid ethyl ester

: 119784-78-0
2-amino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

: 119784-79-1
2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Guidance literature:: for 3h; Heating;
DOI:10.1002/jps.2600770902

Reference yield:

: 119784-74-6
1-benzyloxycarbonyl-4-p-methoxybenzylcarbonylpiperazine

: 119784-79-1
2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / AcOH, HBr / 2 h / 60 °C

2: 61 percent / LiAlH₄ / diethyl ether / Heating

3: 66 percent / 3 h / 80 °C

4: 80 percent / H₂, methanolic NH₃ / Raney nickel / 2 h

5: 48 percent

6: 58 percent / 3 h / Heating

With lithium aluminium tetrahydride; ammonia; hydrogen bromide; hydrogen; acetic acid; nickel; In diethyl ether;
DOI:10.1002/jps.2600770902

Reference yield:

: p-methoxybenzylcarbonylpiperazine hydrobromide

: 119784-79-1
2-carbethoxyamino-N-<2-(4-methoxyphenethyl-1-piperazinyl)ethyl>benzamid

Guidance literature:: Multi-step reaction with 5 steps

1: 61 percent / LiAlH₄ / diethyl ether / Heating

2: 66 percent / 3 h / 80 °C

3: 80 percent / H₂, methanolic NH₃ / Raney nickel / 2 h

4: 48 percent

5: 58 percent / 3 h / Heating

With lithium aluminium tetrahydride; ammonia; hydrogen; nickel; In diethyl ether;
DOI:10.1002/jps.2600770902