1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

Base Information

Chemical Name:1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide
CAS No.:924663-46-7
Molecular Formula:C₁₂H₁₃ClN₂O
Molecular Weight:236.701
Hs Code.:

Synonyms:1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

Suppliers and Price of 1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

Chemical Property:

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Technology Process of 1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

There total 1 articles about 1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 42953-82-2
5,5-dimethylpyrazolidin-3-one

: 924663-46-7
1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

Guidance literature:: In ethanol; at 20 ℃;
DOI:10.1021/ol800904t

Reference yield: 70.0%

: 924663-46-7
1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

: 2495-35-4,25036-21-9
benzylacrylate

: 1437799-76-2
C₂₂H₂₁ClN₂O₃

Guidance literature:: With silver (I) hydrogen carbonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; In 1,2-dichloro-ethane; at 100 ℃; for 16h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201207204

Reference yield:

: 924663-46-7
1-[(2-chlorophenyl)methylene]-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

: 2043-21-2
acryloyl-1,3-oxazolidin-2-one

: (5S,6S)-5-(o-chlorophenyl)-3,3-dimethyl-1-oxo-6-[(2-oxo-3-oxazolidinyl)carbonyl]-tetrahydro-1H,5H-pyrazolo[1,2-a]pyrazole

: (5R,6R)-5-(o-chlorophenyl)-3,3-dimethyl-1-oxo-6-[(2-oxo-3-oxazolidinyl)carbonyl]-tetrahydro-1H,5H-pyrazolo[1,2-a]pyrazole

Guidance literature:: With 4 A molecular sieve; chiral binaphthyldiimine-based ligand; nickel(II) perchlorate; In chloroform; at 20 ℃; for 254h; Title compound not separated from byproducts;
DOI:10.1021/ol062675y