N₄-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine

Base Information

• Chemical Name: N₄-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine
• CAS No.: 1091608-03-5
• Molecular Formula: C₄₅H₅₂N₄O₈Si
• Molecular Weight: 805.015

Synonyms:N₄-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine

Chemical Property of N₄-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine

Chemical Property:

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Technology Process of N₄-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine

There total 1 articles about N₄-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine (1091608-02-4) + benzoic acid anhydride (93-97-0) → N4-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine (1091608-03-5)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1021/jm9013295

Reference yield: 91.0%

N4-benzoyl-5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine (1091608-03-5) → N4-benzoyl-5'-O-(DMT)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine (1091608-04-6)

Guidance literature:

With triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1021/jm9013295

upstream raw materials:

5'-O-(DMT)-3'-O-(TBDMS)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine

benzoic acid anhydride

Downstream raw materials:

N₄-benzoyl-5'-O-(DMT)-2'-N,4'-C-[(N-methoxyamino)methylene]cytidine

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