ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

Base Information

Chemical Name:ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate
CAS No.:177326-62-4
Molecular Formula:C₁₇H₂₁NO₇
Molecular Weight:351.356
Hs Code.:

Synonyms:ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

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Chemical Property of ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

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Technology Process of ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

There total 4 articles about ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 95-92-1
oxalic acid diethyl ester

: 89929-99-7
6-nitro-2-(2-tetrahydropyranyloxy)methyltoluene

: 177326-62-4
ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 0 deg C, 20 min, then rt, 18 h;
DOI:10.3987/COM-96-7396

Reference yield:

: 23876-13-3
(2-methyl-3-nitrophenyl)methanol

: 177326-62-4
ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / p-toluenesulfonic acid hydrate / CH₂Cl₂ / Ambient temperature

2: 85 percent / 60 percent NaH / dimethylformamide / 0 deg C, 20 min, then rt, 18 h

With sodium hydride; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-96-7396

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 177326-62-4
ethyl 2-nitro-6-(2-tetrahydropyranyloxymethyl)phenylpyruvate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / p-toluenesulfonic acid hydrate / CH₂Cl₂ / Ambient temperature

2: 85 percent / 60 percent NaH / dimethylformamide / 0 deg C, 20 min, then rt, 18 h

With sodium hydride; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-96-7396