C₃₇H₃₁N₃O₃S

Base Information

Chemical Name:C₃₇H₃₁N₃O₃S
CAS No.:1261275-88-0
Molecular Formula:C₃₇H₃₁N₃O₃S
Molecular Weight:597.737
Hs Code.:

C<sub>37</sub>H<sub>31</sub>N<sub>3</sub>O<sub>3</sub>S

Synonyms:C₃₇H₃₁N₃O₃S

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Chemical Property of C₃₇H₃₁N₃O₃S

Chemical Property:

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Technology Process of C₃₇H₃₁N₃O₃S

There total 11 articles about C₃₇H₃₁N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 612-35-1
2-Benzylbenzoic acid

: 1261276-98-5
C₂₃H₂₁N₃O₂S

: 1261275-88-0
C₃₇H₃₁N₃O₃S

Guidance literature:: 2-Benzylbenzoic acid; With thionyl chloride; In 1-methyl-pyrrolidin-2-one; for 0.0833333h;

C₂₃H₂₁N₃O₂S; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 0.166667h;

Reference yield:

: 24310-36-9
1-tosyl-2,3,4,5-tetrahydro-1H-1-benzazepin-5-one

: 1261275-88-0
C₃₇H₃₁N₃O₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: trichlorophosphate / 5 h / 20 °C / Reflux

1.2: Cooling with ice

2.1: ethanol; sodium / 0.5 h / Cooling with ice

2.2: 3.5 h / 0 °C / Reflux

3.1: hydrogen bromide; acetic acid / Reflux

3.2: 6 h / Reflux

4.1: pyridine; HATU / 16 h / 20 °C / Inert atmosphere

5.1: pyridine / acetonitrile / 2 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2.33 h / 20 °C / Inert atmosphere

7.1: thionyl chloride / 1-methyl-pyrrolidin-2-one / 0.08 h

7.2: 0.17 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; ethanol; hydrogen bromide; hydrogen; sodium; acetic acid; HATU; trichlorophosphate; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; ethanol; water; acetonitrile;

Reference yield:

: 50998-74-8
methyl N-tosylanthranilate

: 1261275-88-0
C₃₇H₃₁N₃O₃S

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / butanone, 1-

2.1: potassium tert-butylate / toluene

3.1: trichlorophosphate / 5 h / 20 °C / Reflux

3.2: Cooling with ice

4.1: ethanol; sodium / 0.5 h / Cooling with ice

4.2: 3.5 h / 0 °C / Reflux

5.1: hydrogen bromide; acetic acid / Reflux

5.2: 6 h / Reflux

6.1: pyridine; HATU / 16 h / 20 °C / Inert atmosphere

7.1: pyridine / acetonitrile / 2 h / 20 °C / Inert atmosphere

8.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 2.33 h / 20 °C / Inert atmosphere

9.1: thionyl chloride / 1-methyl-pyrrolidin-2-one / 0.08 h

9.2: 0.17 h / 20 °C

With pyridine; hydrogenchloride; thionyl chloride; ethanol; potassium tert-butylate; hydrogen bromide; hydrogen; sodium; potassium carbonate; acetic acid; HATU; trichlorophosphate; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; ethanol; butanone, 1-; water; toluene; acetonitrile;